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Anaerobic purification electrolytic furnace

Release time:2022-08-13  Number of views:577

 

Equipment introduction:


Based on a fully enclosed glove box, the Norbadi anaerobic purification electrolytic furnace provides a stable inert gas protection environment for the vacuum well electrolytic furnace, and the automatic circulation gas purification system ensures a high standard of anaerobic and water-free operating environment.
The equipment is mainly used in molten salt electrolysis to prepare mixed rare earth metals, light rare earth metals lanthanum, cerium, praseodymium, neodymium and rare earth aluminum alloys and other rare earth materials, involving the application of rare earth, semiconductor, nanomaterials, microelectronics and other fields.
  


 

 

 

 



Configuration  

 

Equipment features:

1. Equipped with automatic internal circulating water oxygen purification system to ensure a high standard oxygen-free environment;

2, can achieve vacuum or atmosphere sintering;

3, can achieve rapid sample cooling;

4, ring heating, sample heating more uniform.

Model

NBD-HTGB-4G1215TIRY

Control system

1. 15 temperature curves can be pre-stored to avoid the trouble caused by repeated Settings of different experimental processes;

2. The experiment process is more intuitive and the operation is more convenient;

3.NBD-101E embedded operating system English and Chinese interchangeable graphical interface, 7 inch true color touch screen input, intelligent man-machine dialogue mode, non-linear style temperature correction;

4. It has the functions of overtemperature alarm, broken couple warning, leakage protection and so on.

heating furnace

Intelligent high temperature vacuum well sintering furnace, uniform temperature field, intelligent temperature control operation

Chamber size

Φ150*200mm

Pressure measurement & monitoring

Mechanical pressure gauge with damping oil prevents gauge pointer from being damaged (digital vacuum gauge is optional)

vacuum system

Vacuum degree: ≤5Pa (mechanical pump)

Measuring range

RT—1100℃

Heating rate

30/min,  Recommended heating rate ≤ 10℃/min,

   Main and auxiliary transition chamber and water oxygen circulation purification system

Crucible material

310S

Sample measuring environment

Air environment; Static, dynamic atmosphere environment; Or vacuum environment (≦1000℃)

The heating reaction system is based on the Norbadi intelligent vacuum pit furnace


Cautions 

1. The internal pressure of the gas supply cylinder is high, and when the gas is passed into the glove box, the pressure reducing valve must be installed on the cylinder. It is recommended to choose a small pressure reducing valve for testing, and the measuring range of the pressure reducing valve is 0.01 MPA-0.15 MPa, which will be more accurate and safe in use.

2.310S stainless steel pot long-term use temperature ≦1100℃;

3. When vacuuming, the cover plate of the glove flange should be sealed with the vacuum chamber, and then open the valve on the flange pipe, and then start vacuuming, otherwise the glove will be blown when directly vacuuming;

4. During the heating experiment, always pay attention to the indicator of the pressure gauge. If the absolute pressure gauge reading is greater than 0.15MPa, the exhaust valve must be opened immediately to prevent accidents.

standard configuration

1. One double-station glove box;

2. Vacuum high temperature well sintering system 1 set;

3. 1 set of automatic circulating water oxygen purification system;

4. A copy of the manual.

Service

1 year warranty, lifetime service (warranty does not include consumable parts)

Net weight

500KG


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