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Experimental apparatus for reducing and extracting alloy preparation

Add Time: 2025-02-22    View:1442

The experimental device for preparing alloy by reduction extraction is a high-temperature heating equipment designed specifically for laboratories, mainly used for preparing various alloy materials by reduction extraction method. This heating furnace is capable of conducting reduction reactions and alloying processes of metal oxides in high-temperature environments (usually up to 1200℃), and is suitable for research and development in fields such as materials science, metallurgical engineering, ...

  

Product Details
Application Field
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Equipment features

Precise control: PID temperature control technology and high-precision sensors are used to ensure consistency and repeatability of reaction conditions.
Multi step process integration: Integrating multiple steps such as reduction and extraction into one system to simplify the operation process and improve efficiency.
Efficient Separation: Optimize the extraction process, utilize different physical and chemical properties to achieve effective separation, and reduce impurity content.
High degree of automation: Supports programming control and remote monitoring, allowing users to set process parameters through a computer interface and monitor experimental progress in real-time.
Flexible configuration: Different specifications of reactors, gas flow rates, and other parameters can be customized according to specific experimental needs to meet diverse research needs.

Equipment name

Experimental apparatus for reducing and extracting alloy preparation

power supply

Single phase 220V 50HZ

rated power

6KW (including 2KW molecular pump unit)

heating element

HRE alloy resistance wire

Furnace temperature control accuracy

±1℃

Temperature control sensor (furnace)

K-type thermocouple with a diameter of 2 * 420mm

Temperature control accuracy of reaction kettle

±5℃

Temperature sensor (reactor)

K-type right angle thermocouple with a diameter of 8mm * 100+450

Tmax

1200℃

rated temperature

1150℃

Recommended heating rate

≤20℃/min

Size of furnace temperature zone

φ240*220mm

Sintering crucible size

Outer diameter of 133mm, height of 180mm (at 1100 ℃)

Collect crucible dimensions

Outer diameter of 120, inner diameter of 34.5, height of 30 (at 200-300 ℃)

Molecular pump unit power supply

380V 50HZ

Vacuum pump model

DRV30 KF40 connector extraction speed of 8.3L/s

Molecular pump model

FF-160/620F LF interface with a pumping speed of 600L/s and a speed of 27000 r/min

Overall ultimate vacuum degree of the system

≤5.3×10-4Pa

Furnace body size

Length 1150 * Height 1480 * Depth 700mm

Furnace weight

About 200KG

control system

 

1. Sintering process curve setting: dynamically display the set curve, and the equipment sintering can pre store multiple process curves, each of which can be freely set;
2. Pre order sintering is available to achieve unmanned sintering process curve sintering;
3. Real time display of sintering power, voltage and other information, recording of sintering data, and the ability to export for paperless recording;
4. Capable of remote control and real-time observation of equipment status;
5. Temperature correction: The difference between the main control temperature and the sample temperature is nonlinearly corrected throughout the sintering process.

Appointment sintering

Optimize equipment utilization, ensure sintering process stability, save waiting time, and achieve efficient and orderly sample preparation.

Nonlinear temperature correction

By using algorithms to nonlinearly correct the temperature deviation between the control point and the sample due to their different positions in the temperature field, the consistency between the control temperature and the sample temperature is improved, the operation is simplified, and the accuracy of experimental data is enhanced.

remote control


You can log in to the control system anytime and anywhere through computers, mobile phones, and other terminals to view the operating status of the heating furnace (temperature, pressure, heating rate, etc.), and remotely adjust parameters and start/pause programs according to experimental needs. No need to travel back and forth to the laboratory at night or on holidays to meet the parameter tuning needs during the experimental process; Real time monitoring of key experimental processes can also be achieved during cross regional business trips, significantly reducing ineffective commuting time and allowing researchers to allocate work energy more efficiently.

data storage

Ensure data security, integrity, standardized management, and efficient retrieval

Multiple sets of exclusive process programs can be pre-set


Multiple types of experiment specific temperature programs can be preset to ensure experimental repeatability and ease of operation, support process optimization and data tracing, adapt to team collaboration and technical inheritance, greatly improving experimental efficiency and design flexibility.

heating element

 

HRE alloy resistance wire

condenser

 

The condenser collector is made of 304 stainless steel material and has a built-in water-cooled structure. It condenses the metal vapor brought out by the molecular pump or airflow, reduces the temperature of the reaction mixture, and prevents the generation of by-products. Avoid causing damage to the molecular pump unit.

Equipment usage precautions

1.When the furnace temperature of the equipment is ≥ 300 ℃, it is forbidden to open the furnace to avoid injury;

2.Minor cracks caused by continuous use of the furnace are a normal phenomenon and do not affect the normal use of the equipment;

Service Support

One year limited warranty with lifetime support (warranty does not include consumable parts)

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Address:No. 181 Zhengxin Road, Xinzheng City, Zhengzhou, Henan Province