Configuration details (glove box + series products)

| Equipment characteristics: 1. Simple: user-friendly design operation window, 2. Intelligent HMI man-machine interface, easy to operate; 3. Safety: high sealing fully protects the safety of human body and samples; 4. High efficiency: integrated design improves equipment use efficiency; Energy saving: frequency conversion control operation. 5. Heating, pressure and other heat treatment equipment can be modified according to customer requirements. |

| Major component 1. Main box 2. Purification system 3. Solvent system 4. Water cooling 5. Large transition cabin 6. Small transition cabin 7. Control system
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| Control system 1. Cycle cycle: start and stop cycle purification system; 2. True empty pump: start and stop vacuum pump; 3 lighting: open, take care of the lamp; 4. Analyzer: control water oxygen analyzer; 5. Cleaning: Set details of cleaning parameters; 6. Tacit value: restore the default value set by the system; 7. Alarm setting: set water oxygen alarm prompt; 8. Settings: alarm Settings and leak detection Settings of the box, switch between Chinese and English; 9. Regeneration: press the regeneration key to control the purification column for regeneration; 10. Time setting: preset touch screen display time; 11. Record: query system operation record and water oxygen content record;
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| Transition cabin construction 1. Support frame; 2. Support rod; 3. Large hatch cover; 4. Large cabin shaft; 5. Large transition beam; 6. Handle; 7. Lead screw 8. Hook; 9. Vacuum pressure gauge; 10. Small hatch door; 11. Small hatch handle 12. Three-way ball valve;
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| Replacement of activated carbon
① vacuum gauge; ② three-way ball valve; (3) feeding port; (4) discharge port; Specific replacement process: 1. Close the two butterfly valves on the solvent column (butterfly valve ② and butterfly valve ③ in 10.2); 2. Check whether ① (vacuum gauge) is under normal pressure. If it is under vacuum state, supplement air to normal pressure through ② (three-way ball valve) 3. Open ③ (feeding port) and ④ (discharging port); 4. Activated carbon flows out from ④ (discharge port); Tighten the clamp after cleaning; 5. Pour clean and dry activated carbon from ③ (feeding port); After installation, tighten the clamp; 6. Through the operation of ② (three-way ball valve), vacuum the solvent column and replenish air for three times. 7. Repeat 5.11.2 to flow the circulating gas through the solvent column.
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Electrical specification | AC220V 6KW*2 |
Preparation and inspection before use
| 1. Prepare sufficient high purity working gas (please refer to Table 1 for gas specifications) 2. Prepare two 40L cylinders of recycled gas (gas specifications refer to Table 2 below) 3. Second pair of decompression table (one is used normally, the other is used again)
use | Clean the box, balance the pressure and work gas | Gas type | Nitrogen, argon or helium | purity | 99.999% H2O ≤5ppm; O2 ≤5ppm or better | quantity | Meet the requirements of the equipment | Demand pressure | 0.4-0.6MPa | Pressure gauge range | Main surface pressure range >15MPa; Sub-surface pressure range ≤ 1MPa | Connecting pipe | Material: Plastic; External diameter: ¢10mm; Inside diameter: ¢6.5mm; | Table 1 High purity working gas |
use | Reduction purification column purification capacity | Gas type | When nitrogen is used as the working gas, nitrogen/hydrogen mixture (90-95% N2, 5-10% H2) is used; When argon is used as the working gas, argon/hydrogen mixture (90-95% Ar, 5-10% H2) is used; When helium is the working gas, use a helium/hydrogen mixture (90-95% He, 5-10%H2).
| purity | 99.999% H2O ≤5ppm; O2 ≤5ppm Or better | quantity | Each column requires 3500L or close to 40L cylinders of 10MPa gas pressure | Demand pressure | 约 0.01-0.03MPa | Pressure gauge range | Main surface pressure range >10MPa; Sub-surface pressure range < 0.5MPa | Connecting pipe | Material: Plastic; External diameter: ¢10mm; Inside diameter: ¢6.5mm; | Table 2 Regenerated gas |
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Operation precautions | 1. Personnel shall not use the glove box without training; 2. Prohibit the use of materials that can poison the regeneration catalyst, such as: sulfhydryl compounds, etc. 3. Do not use volatile solvents that will damage plexiglass, such as acetone, without permission; 4. Before using volatile solvent, contact the person in charge to unload the water probe; 5. Open the activated carbon circulation system when using volatile solvent; 6. When using the glove box, do not have long nails, do not wear sharp objects (such as watches, jewelry, etc.);
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