Ultra high pressure and high temperature sintering furnace

Release time: 2025-03-29 17:10:38  Number of views: 561

Ultra high pressure and high temperature sintering furnace is a device specially designed for chemical reactions under extremely high pressure and temperature conditions, widely used in fields such as chemical engineering, pharmaceuticals, and materials science. This device can withstand extremely high working pressure and provide precise temperature control to ensure efficient chemical reactions under extreme conditions. Ultra high pressure reactors are suitable for experiments and production processes that require high-temperature and high-pressure environments, such as supercritical fluid extraction, hydrogenation reactions, polymerization reactions, etc.

Application areas:
1. Chemical industry: used for synthesizing ammonia, hydrocracking, carbonylation reactions, etc.
2. Pharmaceutical: Used for drug synthesis, active ingredient extraction, etc.
3. Materials Science: Used for the synthesis of nanomaterials and functional materials.
4. Research and Education: Suitable for universities, research institutes, and other research institutions to conduct research and teaching experiments in fields such as chemical engineering and materials science.

5. Food processing: used for supercritical carbon dioxide extraction of essential oils, caffeine, etc.

  

product details
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Equipment features:
High strength structure
High pressure resistant material: Made of high-strength alloy steel, it can withstand extremely high working pressure, ensuring the safety and reliability of the equipment.
Precision sealing: using high-performance sealing materials and sealing technology to ensure no leakage under high pressure, preventing the mixing of external air or leakage of internal media.
2. Precise control system
PID temperature control system: adopting advanced PID temperature control system, supporting multi-stage program control, ensuring high temperature control accuracy and good repeatability.
Real time monitoring: equipped with high-precision temperature sensors and pressure sensors, real-time monitoring of temperature and pressure changes inside the kettle, feedback to the control system for adjustment.
• Over temperature and over pressure protection: Built in over temperature and over pressure protection function to prevent safety accidents caused by temperature or pressure loss of control.
3. Safety design
Multiple protection measures: Built in over temperature and over pressure protection, over-current protection and other multiple safety protection measures ensure safe operation.
Emergency stop function: It can quickly cut off the power supply in case of abnormal situations, ensuring the safety of personnel and equipment.
Leak detection: Equipped with pressure and gas leak detection devices to monitor leaks in real time and ensure safety.
4. Easy to operate
• Touch screen control interface: equipped with a touch screen control interface, supporting data recording and remote monitoring, easy to operate.
• Preset program: Provides multiple preset heating programs and reaction conditions, making it convenient for users to choose appropriate process parameters based on specific needs.

Equipment name

Ultra high pressure and high temperature sintering furnace

Specification and model

NBD-HP900-2090TPI2Y-150N(80Mpa)

power supply

Single phase 220V 50HZ

rated power

7KW

Type of temperature measuring element

K-type thermocouple with a diameter of 2 * 420mm

Main control working temperature

≤1000℃

rated temperature

800℃

Maximum pressure of the chamber

80Mpa(800℃)

Reactor material

310s stainless steel

Furnace material

Alumina fiber insulation refractory material

Furnace space

Φ250*290mm

Effective size inside the furnace tube (maximum sample space)

Φ20*50mm

heating rate

≤5℃/min

Furnace body size

Length, height and depth 1470 * 1350 * 870mm

control system


1. Sintering process curve setting: dynamically display the set curve, and the equipment sintering can pre store multiple process curves, each of which can be freely set;
2. Pre order sintering is available to achieve unmanned sintering process curve sintering;
3. Real time display of sintering power, voltage and other information, recording of sintering data, and the ability to export for paperless recording;
4. Capable of remote control and real-time observation of equipment status;
5. Temperature correction: The difference between the main control temperature and the sample temperature is nonlinearly corrected throughout the sintering process.

Temperature Accuracy

± 1 ℃ (pay attention to the lag time of the sample temperature inside the cavity)

heating element

                     


HRE high-temperature alloy heating wire (distributed around)

SEALING SYSTEM

Made of high-strength alloy steel or special stainless steel, ensuring sufficient strength and rigidity.

Test according to customer requirements


Real time shooting data
furnace tube
The furnace tube is made of high-strength 310S special stainless steel to ensure durability and safety under high pressure and high temperature conditions.

Pressure measurement and monitoring

1. The high-pressure chamber is equipped with a pressure sensor and connected to the control system for real-time display
On the flange of the high-pressure relief solenoid valve, when the air pressure inside the furnace tube is higher than the set pressure value, the solenoid valve will automatically open to release air, and the chamber pressure will be maintained within the set pressure range.

Equipment usage precautions

1) Connect the gas source, air compressor, and booster pump.
2) Open the right cover and place the materials inside. The cavity should be clean and free of debris.
3) Check the oxygen free copper sealing gasket for high temperature deformation, discoloration, etching, holes, impurities, and the sealing surfaces of the left and right flanges for impurities and etching. If necessary, use alcohol to scrub.
4) Close the right cover and tighten the nut with a torque wrench (the torque of the torque wrench can be adjusted to between 130Nm-160Nm normally).
5) Adjust the intake pressure of the steel cylinder (not less than 5Mpa), adjust the driving gas pressure of the air compressor (constant 0.8Mpa), use a booster pump to increase the gas pressure entering the reaction chamber to 50Mpa, and continue for a period of time to ensure that there is no air leakage in the equipment.
6) When cleaning, first turn on the booster pump, then turn on the exhaust valve. Gas flows in and out to flush the cranial cavity for a period of time. After cleaning, close the exhaust valve first, and then turn off the booster pump.
7) Set sintering process (especially target temperature and set pressure).
8) Start sintering.
9) After sintering is completed and heating is stopped, wait for the material to cool to the appropriate temperature (to ensure that the material does not oxidize and is not burned by high temperatures), manually open the exhaust solenoid valve to release the furnace chamber pressure (be careful not to release pressure at high temperatures, as it may cause danger).

net weight

300kg

Service Support

One year limited warranty with lifetime support (warranty does not include consumable parts such as processing tubes and O-rings, please order replacement parts at the relevant product below).

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Sale Service: 0371-6320 2801
                      0371-6320 2805
After-sales service: 0371-6320 2805
MR. CAI: 181-0371-5723
Email : nbd@nbdkj.com
Address:8# zhuyuan, Xinhua subdistrict, Xinzheng, Zhengzhou, China
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