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Thermogravimetric analysis (TGA) and condensation collection systems

Release time:2022-12-19  Number of views:287


Equipment introduction:


This product was developed for the analysis of the weight loss and pyrolysis weight (TGA) of materials during combustion in a vacuum or atmosphere. It includes balance, heating furnace, programmed temperature control system, recording system and other parts, which can observe the change of sample quality with temperature, time, vacuum degree and atmosphere state in the process of heating, constant temperature or cooling, and is equipped with a condensation collection device for pyrolytic substances. Widely used in plastics, rubber, coatings, drugs, catalysts, inorganic materials, metal materials and composite materials and other fields of research and development, process optimization and quality control.


 

 


Configuration

 

Equipment introduction:


1. The furnace body heating adopts ring arrangement to reduce interference;

2. The weighing sensor made of precious metal nickel-chromium alloy has the advantages of high temperature resistance, oxidation resistance and corrosion resistance;
3. The power supply, circulation heat dissipation part and the host are separated to reduce the impact of heat and vibration on the micro-heat sensor;
4. Adopt the upper electric lifting structure, easy to install and operate;

5. Water bath constant temperature device is used to isolate the thermal influence of heating furnace body on the chassis and micro-thermobalance;

6. Built-in circulating water-cooled condensation collection device, which can collect pyrolytic substances more efficiently.

Model

NBD-TGA1100-80TD2ZY5L

main function

1. In the process of heating, constant temperature or cooling, the quality of the sample can be automatically recorded with the change curve of temperature, vacuum, gas flow and time;

2. Measure and study the following properties of materials: thermal stability, adsorption and desorption, quantitative analysis of components, moisture and volatiles, decomposition process, oxidation and reduction, effects of additives and fillers, reaction kinetics;

3. The circulating water-cooled condensation collection device can efficiently condense and collect gaseous substances precipitated by pyrolysis at the same time.

Electrical Spec

AC220V   4.5KW

Tmax

1150 ℃

Temp Accuracy

±1℃

thermocouple

Type K thermocouple 420mm

heating-zone size

φ150*430mm single heating-zone dual control

Furnace tube material

310s Stainless steel tube/quartz (interchangeable)

Load cell range

300g

precision

Within 0.03g

Weight of wire and crucible

Approx.30g

Crucible material&size

Aluminum/stainless steel φ60*30mm

The sample can be weighed

0~270g

Condensing collector volume and height adjustable range

110ml can be moved up and down 60mm

Low temperature constant temperature reaction bath temperature control accuracy

±1 degree volume 6L

Furnace size

L945×D510×H2400mm

Recommended heating rate

≤10℃/min

Control system

 

1. Weighing sensor range: 300g;

2. Temperature curve setting: 15 temperature curves can be pre-stored, and 30 sections of "temperature-time" curves can be set for each;

3. Control mode: PLC to achieve automatic control of transmission mechanism, temperature module, ventilation, vacuum and weighing module;

4. NBD-101EP embedded operating system English and Chinese interchangeable graphical interface, 7 inch true color touch screen input, intelligent man-machine dialogue mode, real-time heating power display, non-linear pattern temperature correction; The experimental report is generated independently, and the experimental data is exported unlimited times.

5. Data interface: USB data interface, support data export U disk and online printing;

6. Transmission mechanism: stepper motor drives ball screw for transmission, which is more stable and more convenient for loading and unloading materials;

7. Data recording method: automatic storage according to the set time interval;

8. Weighing module: Unique weighing module, higher accuracy and stability.

Equipment details

 

 

 

Vacuum degree: ≤10Pa

Pressure measurement and monitoring

 

The mechanical pressure gauge with damping oil is used to make the pressure fluctuation produce damping and reduce the pointer swinging back and forth.

gas supply system

 

Built-in gas mass flowmeter, including two gas switching and flow size control.

net weight

220KG(excluding vacuum pump and water cooling circulator)

Cautions 

1. When the furnace temperature of the equipment is ≥300℃, do not open the furnace to avoid damage;

2. When the equipment is used, the pressure in the furnace tube shall not exceed 0.125MPa (absolute pressure) to prevent damage to the equipment caused by excessive pressure;

3. When used under high vacuum (10 to the minus 3 Pa), the use temperature of the equipment shall not exceed 800℃.

Service

1 year warranty with lifetime support (warranty does not cover consumable components such as furnace tubes and seals). 



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